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Organic Chemistry II

Distillation, melting temperature and working safely

  • 3 things to know
  • Papers 2 and 3

Overview

Simple and steam distillation, judging purity from a sharp or broad melting range, using hazard data to select and justify control measures, the techniques in the aspirin preparation of Core Practical 16, and why Grignard reactions need dry ether.

What you need to know

Answer each one before you reveal it.

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Key term

What solvent is typically used for Grignard reagent reactions and reactions involving carbonyl compounds?

Key term

In distillation, what happens to the mixture in the distillation flask?

Key term

Which component vaporises first during distillation and why?

Questions from this subtopic

Each one with the model answer underneath.

  1. 1

    In distillation, what happens to the mixture in the distillation flask?

    Model answer

    The mixture is heated, causing the more volatile component to vaporise.

  2. 2

    Which component vaporises first during distillation and why?

    Model answer

    The component with the lower boiling temperature vaporises first because it requires less energy to change from liquid to gas.

  3. 3

    What is the function of the condenser in distillation?

    Model answer

    The condenser cools the vapour, converting it back into liquid.

  4. 4

    What is the distillate in a distillation process?

    Model answer

    The distillate is the purified liquid collected after condensation of the vapour.

  5. 5

    In steam distillation, how is steam introduced to the mixture?

    Model answer

    Steam is passed through the mixture containing the compound to be purified.

  6. 6

    What happens during co-distillation in steam distillation?

    Model answer

    The organic compound and water distil together at a temperature below 100°C.

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AAtomisation turns each element into gaseous atoms.
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